Publication: Fabrication and characterization of hydrophilic TiO2 thin films on unheated substrates prepared by pulsed DC reactive magnetron sputtering
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Issued Date
2010
Resource Type
File Type
application/pdf
ISSN
16874110
Other identifier(s)
2-s2.0-77956808686
Rights Holder(s)
Scopus
Bibliographic Citation
Journal of Nanomaterials. Vol 2010, No. (2010), p.-
Suggested Citation
Horprathum M., Chindaudom P., Limnonthakul P., Eiamchai P., Nuntawong N., Patthanasettakul V., Pokaipisit A., Limsuwan P. Fabrication and characterization of hydrophilic TiO2 thin films on unheated substrates prepared by pulsed DC reactive magnetron sputtering. Journal of Nanomaterials. Vol 2010, No. (2010), p.-. doi:10.1155/2010/841659 Retrieved from: https://hdl.handle.net/20.500.14740/7544
Abstract
TiO2 thin films were deposited on unheated silicon wafers (100) and glass slides by a pulsed DC reactive magnetron sputtering in an ultrahigh vacuum (UHV) system. The effects of both an operating pressure and deposition time on film structure, surface morphology, and optical property were studied. The film structure and microstructure were characterized by grazing-incidence X-ray diffraction (GIXRD) technique and transmission electron microscopy (TEM). The surface morphology was investigated by field emission scanning electron microscopy (FE-SEM). The optical property of the TiO2 thin films was determined by spectroscopic ellipsometry (SE). The water contact angle measurement was also used to determine hydrophilicity of the films after exposed to UV light. The results suggested that the TiO2 thin film at less than 40nm was amorphous. As the thickness was increased, the mixture of anatase and rutile phases of TiO2 began to form. By reducing the operating pressure during the film deposition, the rutile phase component can also be enhanced. Both the increased film thickness and decrease operating pressure were the critical factors to improve the hydrophilicity of the TiO2 thin films. Copyright © 2010 M. Horprathum et al.
Subject(s)
Critical factors
Deposition time
Field emission scanning electron microscopy
Film deposition
Film structure
Glass slides
Grazing-incidence X-ray diffraction
Operating pressure
Pulsed DC
Rutile phase
Rutile phasis
TEM
TiO
Unheated substrates
UV light
Water contact angle measurement
Amorphous films
Angle measurement
Contact angle
DC power transmission
Field emission
Field emission microscopes
Hydrophilicity
Morphology
Optical properties
Oxide minerals
Scanning electron microscopy
Silicon wafers
Spectroscopic ellipsometry
Surface morphology
Thin films
Titanium dioxide
Transmission electron microscopy
Vapor deposition
X ray diffraction
Semiconducting silicon compounds
Deposition time
Field emission scanning electron microscopy
Film deposition
Film structure
Glass slides
Grazing-incidence X-ray diffraction
Operating pressure
Pulsed DC
Rutile phase
Rutile phasis
TEM
TiO
Unheated substrates
UV light
Water contact angle measurement
Amorphous films
Angle measurement
Contact angle
DC power transmission
Field emission
Field emission microscopes
Hydrophilicity
Morphology
Optical properties
Oxide minerals
Scanning electron microscopy
Silicon wafers
Spectroscopic ellipsometry
Surface morphology
Thin films
Titanium dioxide
Transmission electron microscopy
Vapor deposition
X ray diffraction
Semiconducting silicon compounds
